Problem: Sample carryover
Possible Cause(s): Insufficient number or type of washes Solvent wash vial empty Syringe worn or dirty Sample/solvent mismatch Dirty ALS needle guide Suggested Action(s): Increase number or type of washes Rinse with a variety of solvents Rinse and refill solvent wash vial Clean or replace syringe Ensure samples and solvents, from one vial to the next, are miscible Replace needle guide
Possible Cause(s):
Insufficient number or type of washes
Solvent wash vial empty
Syringe worn or dirty
Sample/solvent mismatch
Dirty ALS needle guide
Suggested Action(s):
Increase number or type of washes
Rinse with a variety of solvents
Rinse and refill solvent wash vial
Clean or replace syringe
Ensure samples and solvents, from one vial to the next, are miscible
Replace needle guide
More....