David wrote:I would check a few things:
- what is the vacuum
- Could you tune the system in EI
- when is the last time you cleaned the source
- what does air/water look like
- can you adjust the methane flow?
- try deleting the tune file
- what is the column flows
- do you have adequate methane pressure
- what is the quality of methane
- did it work before
- what is the vacuum
[6 x 10(-5)]- Could you tune the system in EI
[Yes]- when is the last time you cleaned the source
[Brand New, never been used]- what does air/water look like
[EI- N2 <2%]- can you adjust the methane flow?
[Yes]- try deleting/rebuilding from default the tune file
[Tried that]- what is the column flows
[1 ml/min]- do you have adequate methane pressure
[Yes]- what is the quality of methane
[Reagent Grade, using on a another system]- did it work before
[Yes]